Clinical Chemistry
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Clinical Chemistry 22: 221-223, 1976;
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Clinical Chemistry, Vol 22, 221-223, Copyright © 1976 by American Association for Clinical Chemistry

Rapid micromethod for blood lead analysis by anodic stripping voltammetry

G Morrell and G Giridhar

We describe a rapid microscale procedure for blood lead determination by anodic stripping voltammetry. Results correlate well with those obtained by atomic absorption spectroscopy. The procedure involves use of a metal-exchange reagent, which rapidly releases bound lead from its macromolecular binding sites, thus eliminating a long and cumbersome perchloric acid digestion procedure. Reproducibility and analytical recovery of added lead were both excellent. Our results show that anodic stripping voltammetry is a reliable, sensitive micromethod for routine determination of blood lead.


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Copyright © 1976 by the American Association for Clinical Chemistry.