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Clinical Chemistry 24: 1720-1723, 1978;
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Clinical Chemistry, Vol 24, 1720-1723, Copyright © 1978 by American Association for Clinical Chemistry

Negative-ion mass spectrometry of amphetamine congeners

Y Marde and R Ryhage

Negative-ion chemical ionization mass spectrometry with a conventional combined gas chromatograph-mass spectrometer has been used for the analysis of amphetamine-like compounds. Ammonia was used as the reagent gas, which gives rise to few but specific sample-fragment ions, such as (M--1)- as the base peak, m/z 91, and a smaller peak corresponding to the end part of the side chain. Five reference compounds and a urine sample from an overdose case were analyzed. Comparative positive-ion chemical ionization reference spectra were also recorded.




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Copyright © 1978 by the American Association for Clinical Chemistry.