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Clinical Chemistry 24: 483-485, 1978;
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Clinical Chemistry, Vol 24, 483-485, Copyright © 1978 by American Association for Clinical Chemistry

Quantitation of anticonvulsant drugs in serum by gas-chromatography on the stationary phase SP-2510

W Godolphin and J Thoma

A new column packing, SP-2510 DA (Supelco, Inc., Bellefonte, Pa. 16823), is an excellent stationary phase for the determination of a wide variety of anticonvulsant drugs by gas--liquid chromatography without derivatization. However, when uncomplicated extraction procedures are used, serum cholesterol interferes with the determination of primidone. By the simple expedient of adding a short "pre-column" containing another phase (SP-2250 DA) the problem is overcome.




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Copyright © 1978 by the American Association for Clinical Chemistry.