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Clinical Chemistry 5: 45-49, 1959;
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Clinical Chemistry, Vol 5, 45-49, Copyright © 1959 by the American Association for Clinical Chemistry

Determination of Magnesium and Calcium in Urine

Raul Carubelli 1, William O. Smith 1, and James F. Hammarsten 1

1 Medical and Radioisotope Services, V. A. Hospital, the Oklahoma Medical Research Foundation, and the Department of Medicine, University of Oklahoma School of Medicine, Oklahoma City, Okla.

A procedure for the determination of both calcium and magnesium in urine is described.

The method consists of the separation of calcium from magnesium and individual spectrophotometric titrations of each using EDTA as a complexometric reagent and murexide and eriochrome black T as indicators.

Recoveries have proven very satisfactory.

Submitted on September 23, 1958






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Copyright © 1959 by the American Association for Clinical Chemistry.